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Red Devil has been pulled off the shelves in the USA.You probably won't see it unless somebody has a large backstock of it.There are still other options for pure NaOH out there.Lots of places online to purchase it.

Grateful Dead~Truckin'~10/19/72~The Fox Theatre,St.Louis,MO

Grateful Dead~Smokestack Lightning~2/13/70~Fillmore East,New York,NY

Grateful Dead~Dark Star~10/12/68~Avalon Ballroom~San Francisco,CA

Here is another tek I have on my hard drive.Hope it comes in handy for someone not wanting to work with as much material at one time.


<<<<<<<<<<<<"TEK 100">>>>>>>>>>>>>>>>>>
Grind 100g of MHRB to fine powder using a glass blender.
Mix solution: 1/4 pint of White (5%)Vinegar to 28oz of Distilled Water.
Place in a 1.5L glass topped Crockpot & add the solution till MHRB is completly submerged, then turn on crockpot.
Use the rest of the solution for your second extraction.
2 extractions / each for 2 hrs. (afterwards clean crockpot for Hot Water Bath).
When you strain the second extraction press the plant fiber out into the container.
Strain both extractions in to large plastic container & place into the frig for 2 hours. This is called Cold filtering.
once both extractions are cold filtered, strain the red fluid into a 750ml bottle.
At the bottom of the cold plastic container you'll see gummy brown sediment, throw that away.
Now heat up your crockpot for the Hot water bath.
Use a small glass bottle & Basify with 1Tbsp Lye to 150ml Warm water.
Now add to your 750ml bottle & upend Slowly till it's all BLACK in color.
(turn cap to release pressure after each upending)
Leave about an inch at the neck of the 750ml bottle for your Naptha.
For each extraction place a small bottle filled with approx. 100ml Naptha in Hot water bath, get it good & hot. place the small bottle next to the 750ml bottle in the hot water bath.
(leave cap slighty loose to release pressure).
Then add & upend 30ml HOT naptha to the 750ml bottle.(release pressure each time) upend the bottle for a few minutes & Place in hot water bath. I've seen it seperate in 10 minutes when good & hot. Do three 30ml hot naptha extractions. Once seperated use a pipette or better yet an eye dropper to extract the naptha containing your spice.
Put all naptha extractions in small sealed mason jar, (first use a small glass to catch any black goo that might get in, that way you can remove it before adding to your mason jar).
Freeze sealed jar overnite till white crystal flakes have completely fallen out of solvent. Thoroughly dry flakes on coffee filter in funnel in cup. (you can save the solvent for further extractions). Final cold filter wash, chill a nip bottle mixed with 50% Clear ammonia / 50% Distilled water, slowly pour just a little over dry product on filter, then Fully Dry to room temperature. Keep the product in a cool dry place otherwise it may melt in the summer heat.

End Results for 100g: "The 750ml bottle should produce 570mg spice"

I found this at another also thought it was very interesting.Anybody have any experience with this?


                             Jungle DMT
 

 
I once posted this in another place and thought there might be some interest in it here. Before Vovin's Forum went down, a TEK was posted that showed how to extract another, previously unknown, alkaloid from Mimosa Hostilis. The other alkaloid was extracted and formed RED crystals that were insoluble in naptha. Smoking tests of the red crystals showed it to be more powerful than DMT and resulted in a less comfortable trip described as "darker and scary". Although there was a spirited discussion of what it could be, there was no general consensus on what it was, and the best opinion seemed to be that it was some form of beta-carboline. I was emailed this TEK at the time by the author (Critical Switch), and still have it on my hard drive. Critical Switch's original purpose in using a xylene/naptha extraction sequence was to maximize DMT extraction yields. He said that xylene would pull everything out of the Mimosa, then the dried product was washed with naptha to remove the DMT. Claimed an extra 15% DMT yield. However, his xylene/naptha sequence after the naptha wash left a red crystalline residue behind. Always the adventurous soul, he tried smoking the red crystals and got a dark scary trip MUCH stronger than DMT. He called it "Jungle DMT". It was throughly discussed on Vovin's Forum, with no clear consensus of what it could be. Possibly a beta-carboline. Although I have the entire TEK on my hard drive, here are some pix of the parts where he extracted the red crystals. The best thing about it is that in the usual process of extracting DMT from Mimosa, it would normally be thrown away with the fiber. This process extracts BOTH alkaloids. DMT and the "other". The easiest way to do this is to use xylene for the nonpolar extraction and evaporate it with a small fan to a brown powder. Grind up the powder with a mortar and pestle. Then the brown powder is washed on coffee filter paper with naptha. The naptha is retained for freeze-precipitation of the DMT, and what remains on the filter paper is dried out to form bright red hallucinogenic crystals. Stronger than DMT. Comments?

This used to be posted at another forum.Enjoy.


 Heraclitus' Recrystallisation Tek


DMT Recrystallization for Beginners:

Recrystallization is an art. There are as many ways to recrystallize as to paint a picture. This is an easy way to recrystallize dmt, but it is by no means the best or only way. This procedure uses naptha because it's commonly available to people working with dmt, but solvents like heptane or hexane work even better.

1. Add 20 to 25ml of naptha per gram of dmt to a glass container. A small flask or beaker is ideal. Then add the dmt.

2. Heat the beaker to 40 or 50C. A pot of recently boiled water is plenty hot. (NO FLAMES OR SPARK SOURCES AROUND NAPTHA)

3. After a minute or two of heat, the dmt should melt and mostly dissapear in to solution. Very often a mass of yellow/orange goo will sit on the bottom and refuse to go in to solution. If at this point the naptha goes yellow, let it cool for a little while and the yellowness should fall out leaving the naptha clear.

4. Carefully pour as much clear naptha off the insoluble junk as you can in to another container. This container must be something that you can recover crystals from later. (optional - while transferring from one container to another, pour the solution through a very small filter of some sort. a bit of cotton ball in a funnel for example)

5. Add another 5ml or so of naptha to the original container, and add heat again. Again pour off as much clear naptha as possible in to the other container.

6. Cool the clear naptha as slowly as possible. Let it at room temperature for a few hours. Crystals should begin to precipitate. (optional - you could add a few seed crystals for better crystal formation) Then stick it in the fridge or freezer for at least a few hours.

7. While the beaker is very cold, pour the naptha off the crystals. Freezer temperature naptha holds very little dmt, but feel free to evaporate it to make sure.

8. (optional - Scrape the crystals in to a coffee filter, and pour 10 or 20ml of very cold water over them.)

And that's it. Repeat as desired.

It's important to remember that not all naptha is created equal, and your naptha may dissolve more or less than 1g per 25ml. If signficant amounts of dmt are left in the original container after you do this process (more than 100mg), use slightly more solvent next time.
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Yes I think most know it is not at dmtworld anymore.It can be found on a couple other forums I have seen.So now it's here and hopefully some people can put it to good use. It works great.

Grateful Dead~Doin' That Rag~3/2/69~Fillmore West~San Francisco,CA

[How to easily make DMT]

How to easily make DMT:
=======================
Break 1-Pound of Mimosa Hostilis rootbark into 1" pieces using new heavy-duty
wirecutters, then grind it all up in a glass-topped blender, a little at a time.
------------------------------------
Polar Extraction: Premix in an empty 1-Gallon plastic jug: 1-Quart White Vinegar
& 3-Quarts Water. Put the ground up Mimosa in a 3-Liter crockpot, then fill it
with the water-vinegar solution. Stir well and turn it on "high". After 2 hours,
remove the crockpot ceramic liner, hold the lid on slightly offset, and pour off
most of the liquid into a 1-gallon wide-mouthed glass or stainless container.
Add the remaining water-vinegar solution to the crockpot again. Stir well and
turn it on "high". After 2 hours, remove the crockpot ceramic liner, hold the
lid on slightly offset, and pour off all of the liquid into the same container
again. Discard the rootbark fiber and save the two combined extractions in the
1-gallon container. Allow the vegetable particles in the extraction in the
1-gallon container to settle to the bottom overnight. Then pour off the liquid
into an empty 1-Gallon glass wine jug, being careful not to pour off any of the
vegetable sludge at the bottom. Discard the sludge and keep the contents of the
wine jug.
------------------------------------
Basification: Premix in advance a solution of: 5 heaping Tablespoons (70grams)
of Lye (Lowes Hardware, item# 146450 "Roebic Crystal Drain Opener") SLOWLY
added to 1-Pint of warm water. Stir well. Slowly add this solution to the jug,
then cap it. Gently tilt the wine jug back and forth for 1 full minute to mix.
------------------------------------
Nonpolar Extraction: Add 250ml of (Ace Hardware) VM&P Naptha to the wine jug. Then add exactly enough warm water to the jug to raise the liquid level to an inch below the top. Cap the jug. Gently tilt the wine jug slowly back and forth for 5 full minutes to mix the contents. Allow the jug to sit undisturbed on a table for at least 4 hours. There should now be two layers visible in the jug,
a lower dark one and a smaller clear one on top filling the neck of the jug.
Use a glass turkey baster to suck up the top clear layer into a pint mason jar.
Be careful NOT to suck up any of the lower brown foam/black liquid layer into
the mason jar.
-------------------------------------
Freeze-precipitation/wash: place the sealed mason jar in a FREEZER for 3 days
to precipitate the crystals. Prepare a filter setup by placing a funnel into
a quart mason jar and putting a small coffee filter paper into the funnel.
Shake the naptha in the mason jar strongly to stir up all the crystals at the
bottom and quickly pour while still very cold into the funnel for filtering.
Impure yellow-white DMT crystals will be seen on the coffee filter paper.
Allow the crystals to completely dry out on the filter paper in the funnel.
Chill a bottle of NON-SOAPY clear Ammonium Hydroxide(Ace Hardware Janitorial
Strength Ammonia) in a refrigerator. Slowly pour 35ml of the cold ammonia over
the crystals (still in the filter paper) to wash them. Remove the filter paper
from the funnel, spread it out flat and allow the crystals to COMPLETELY dry out.
You will now have 2-1/2 grams of white crystal DMT. Mix it with some dried
parsley and smoke a little in your favorite pipe!...Marsofold
=================================================
Optional Tips:
#1 Grind the rootbark up to 1mm diameter or smaller. Finer is better.
#2 Use three water-vinegar extractions rather than two. Divide up the
water-vinegar mix so that you roughly use 50% for the first extraction,25% for
the second, and 25% for the third extraction. After the last extraction press
out the fiber to squeeze the last bit of liquid from it.
#3 Basify to a ph of 13. Underbasification is the most common reason for a poor
yield. If you don't have ph papers, basify till it turns black, then add an
additional 25% of whatever amount of basification solution you used. This is to
guarantee that you're at a ph of 13. The brown foam you see floating on top of
the basified extract after tilting the jug should flatten out to a thickness of
no more than 1/2" after 45 minutes or so if you've used enough lye.
Add a bit more lye and re-tilt the jug to mix if it's thicker than that.
#4 Naptha: Dividing the naptha amount into two "pulls", then combining them into the same mason jar for freezing will raise the yield by 10%. The best way of extracting if you aren't sure of the yield is to use a slight excess to extract
and evaporate it down with a small fan to 1/3 of the original volume. THEN freeze it. This will pretty much guarantee excellent results. For example: For a pound of rootbark use 300 milliliters of naptha to extract. Evaporate it down to
100 milliliters. Then freeze it and filter out the crystals. You must very quickly filter it within a minute or two after removal from the freezer so that it doesn't have any time to warm up. And your freezer can't be marginally cold. If it doesn't freeze ice cream HARD, then it isn't cold enough.
#5 A small marble in the naptha rattled around in the mason jar will loosen up
the crystals for filtering. It won't hurt anything to pour it out with the crystals into the filter paper. A buchner funnel is the best kind for filtering.
#6 Washing: Be sure that the crystals are absolutely DRY before washing.
Weigh them and use 14ml of chilled ammonium hydroxide per gram of crystals.